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All of the above niclosamide particles (AK Sci, Sigma as supplied, precipitated, converted and recrystallized) would now require crystallographic analyses for measuring polymorphic, hydrate, and amorphous states as could be done by x-ray crystallography and/or FT-IR/Raman, as well as calorimetric evaluation, as used here for two polymorphic forms of sulindac with very different solubilities (76)

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